Triphenylphosphine → HCID 86753397, compound

Participants

Reaction Steps

3.38 g of 4-chloro-2-methoxymethoxybenzyl chloride [prepared as described in step (c) above] were dissolved in 50 ml of toluene, and then 6.02 g of triphenylphosphine were added to the resulting solution. The resulting mixture was heated under reflux for 15.5 hours. At the end of this time, the reaction mixture was cooled on ice, and the crystals which precipitated were collected by filtration, and dried in vacuo, to give 6.02 g (yield 82%) of the title compound.

Provenance & Evidence