HuagongsheHuagongshe Chemistry Print Report · For research reference only
((2(5)-Benzoylamino-3-methylbutyryl)-(3-methanesulfonylbenzyl)amino)acetic Acid Ethyl Ester → 3(S)-(2-((2(S)-Benzoylamino-methylbutyryl)-(3-methanesulfonylbenzyl)amino)acetylamino)-4-oxo-butyric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ((2(5)-Benzoylamino-3-methylbutyryl)-(3-methanesulfonylbenzyl)amino)acetic Acid Ethyl Ester | HCID 53767326 | — |
| Reactant | 3(S)-(2-((2(S)-Benzoylamino-3-methylbutyryl)benzylamino)acetylamino)-4-oxo-butyric Acid | HCID 54405243 | — |
| Reactant | ((2(S)-Benzoylamino-3-methylbutyryl)-(3-Bocaminobenzyl)amino)acetic Acid Ethyl Ester | HCID 54548631 | — |
| Product | 3(S)-(2-((2(S)-Benzoylamino-methylbutyryl)-(3-methanesulfonylbenzyl)amino)acetylamino)-4-oxo-butyric Acid | HCID 87966200 | — |
Reaction Steps
Compound 745 was prepared by a method similar to the method used to prepare compound 706, except compound 703 was replaced with compound 744. 1H NMR (CD3OD) δ 8.29 (m), 8.02 (m), 7.82-7.69 (m), 7.51-7.32 (m), 7.29-7.01 (m), 6.98 (d), 4.94-4.38 (m), 4.36 (d), 4.34 (d), 4.30-4.13 (m), 4.04 (d), 3.31-3.19 (m), 2.88-2.77 (m), 2.64-2.48 (m), 2.44-2.32 (m), 2.21 (m), 1.00-0.83 (m). ##STR124##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843904 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-72ccb4a805a14ab1833d7eb6cecabe40 |
| Source note | uspto-grants-1998_12 |