Magnesium Acetate → HCID 70230036, compound

HRID 1456833Notes

Reaction equation

HRID 1456833 reaction equation
O[CH:2]([N:18]1[C:22](=[O:23])[CH2:21][CH2:20][C:19]1=[O:24])[C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH:9](O)[N:10]2[C:14](=[O:15])[CH2:13][CH2:12][C:11]2=[O:16])[CH:4]=1.[C:25]([O-:28])(=O)[CH3:26].[Mg+2].[C:30]([O-])(=[O:32])[CH3:31]>C(OC(=O)C)(=O)C>[C:30]([CH:2]([N:18]1[C:22](=[O:23])[CH2:21][CH2:20][C:19]1=[O:24])[C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH:9]([C:25](=[O:28])[CH3:26])[N:10]2[C:14](=[O:15])[CH2:13][CH2:12][C:11]2=[O:16])[CH:4]=1)(=[O:32])[CH3:31]

Participants

4

Reactant 2

HCID 8896Magnesium AcetateHCID 70232074HCID 70232074, compound

Product 1

HCID 70230036HCID 70230036, compoundYield 16,670.1%

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Conditions

Temperature
100 °C

Procedure

A mixture of 10 g 1,3-bis(hydroxysuccinimidomethyl)benzene, 20 mg magnesium acetate and 50 ml acetic anhydride was heated at 100° C. for 1 hour. The acetic anhydride and acetic acid were evaporated under reduced pressure, leaving 9 g (72%) of a light brown crystalline product.

Workup

  1. customThe acetic anhydride and acetic acid were evaporated under reduced pressure

Sources & evidence

ORD record
ord-50c110aefc3e4ce486cfc65a27779afe
Source dataset
uspto-grants-1998_12
Patent number
US05844049

Reaction notes

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