HRID1456833

反应详情

EQUATION

反应方程式

HRID 1456833 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

A mixture of 10 g 1,3-bis(hydroxysuccinimidomethyl)benzene, 20 mg magnesium acetate and 50 ml acetic anhydride was heated at 100° C. for 1 hour. The acetic anhydride and acetic acid were evaporated under reduced pressure, leaving 9 g (72%) of a light brown crystalline product.

WORKUP

后处理

  1. customThe acetic anhydride and acetic acid were evaporated under reduced pressure