Chlorosuccinimide → HCID 15817628, compound

HRID 1456845Notes

Reaction equation

HRID 1456845 reaction equation
[Cl:1]N1C(=O)CCC1=O.Br[C:10]1[C:18]2[C:17]([O:19][CH3:20])=[N:16][C:15]([NH:21]C=O)=[N:14][C:13]=2[N:12]([C@@H:24]2[O:34][C@H:33]([CH2:35][O:36][C:37](=[O:41])[CH:38]([CH3:40])[CH3:39])[C@@H:26]([O:27][C:28](=[O:32])[CH:29]([CH3:31])[CH3:30])[CH2:25]2)[CH:11]=1>C(#N)C.CN(C=O)C>[Cl:1][C:10]1[C:18]2[C:17]([O:19][CH3:20])=[N:16][C:15]([NH2:21])=[N:14][C:13]=2[N:12]([C@@H:24]2[O:34][C@H:33]([CH2:35][O:36][C:37](=[O:41])[CH:38]([CH3:40])[CH3:39])[C@@H:26]([O:27][C:28](=[O:32])[CH:29]([CH3:31])[CH3:30])[CH2:25]2)[CH:11]=1

Participants

4

Reactant 2

HCID 31398ChlorosuccinimideHCID 15218405HCID 15218405, compound

Product 1

HCID 15817628HCID 15817628, compound

Reagents, catalysts & solvents 1

HCID 21891449acetonitrile N,N-dimethylformamideSolvent

Procedure

Using N-chlorosuccinimide, the substance was prepared and worked up in analogy with compound (19). The halogenation reaction time was 8 hours. Acetonitrile/DMF (4:1) was used as the solvent. Colorless solid (70%).

Workup

  1. customthe substance was prepared
  2. customThe halogenation reaction time

Sources & evidence

ORD record
ord-5c478d439f0a4c46a64f1cc770dc8890
Source dataset
uspto-grants-1998_12
Patent number
US05844106

Reaction notes

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