HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isonicotinoyl chloride hydrochloride → HCID 15428633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isonicotinoyl chloride hydrochloride | HCID 12262826 | — |
| Reactant | HCID 21221611 | HCID 21221611 | — |
| Product | HCID 15428633 | HCID 15428633 | 36% |
Reaction Steps
Beginning with 0.100 gm (0.30 mMol) of (+)-N,N-dimethyl-8-(tert-butoxycarbonyl)amino-1,2,3,4-tetrahydro-2-dibenzofuranamine and 0.100 gm (0.56 mMol) of isonicotinoyl chloride hydrochloride, 0.036 gm (36%) of the title compound were recovered in two crops from toluene/hexane by the procedure described in Example 24.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05846995 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-2b6f36dba5ae4179ad24c8ba567e7c13 |
| Source note | uspto-grants-1998_12 |