Methylamine → HCID 69947338, compound

HRID 1457075Notes

Reaction equation

HRID 1457075 reaction equation
[CH3:1][N:2]([CH3:19])[CH:3]1[CH2:18][CH2:17][C:6]2[O:7][C:8]3[CH:13]=[CH:12][C:11]([C:14](Cl)=[O:15])=[CH:10][C:9]=3[C:5]=2[CH2:4]1.[CH3:20][NH2:21]>>[CH3:20][NH:21][C:14]([C:11]1[CH:12]=[CH:13][C:8]2[O:7][C:6]3[CH2:17][CH2:18][CH:3]([N:2]([CH3:19])[CH3:1])[CH2:4][C:5]=3[C:9]=2[CH:10]=1)=[O:15]

Participants

3

Reactant 2

HCID 6329MethylamineHCID 21221671HCID 21221671, compound

Product 1

HCID 69947338HCID 69947338, compoundYield 21.1%

Procedure

Beginning with 0.011 gm (0.04 mMol) 2-dimethylamino-1,2,3,4-tetrahydrodibenzofuran-8-carbonyl chloride and 0.08 mMol methylamine, 0.0023 gm (20%) of the title compound were recovered.

Sources & evidence

ORD record
ord-5d171d570d3b4f31aa991ac288fba12f
Source dataset
uspto-grants-1998_12
Patent number
US05846995

Reaction notes

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