HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86195276, compound → HCID 21997027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86195276 | HCID 86195276 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 21997027 | HCID 21997027 | — |
Reaction Steps
A mixture of 2-[(n-butylsulfonyl)methyl]-3-(n-butylsulfonyl)-propanoic acid, ethyl ester (1.0 g, 3.0 mmol) in 6N hydrochloric acid (20 mL) is refluxed overnight. The mixture is transferred to distilled water and extracted with ethyl acetate. The combined organic extracts are concentrated in vacuo to yield the title compound as a clear, colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05847153 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-4c799b1092114cd192fb2d239ccb9b83 |
| Source note | uspto-grants-1998_12 |