HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 3610739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Glycine | HCID 750 | — |
| Reactant | 2,5-Dichloronitrobenzene | HCID 6977 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Diethylene Glycol | HCID 8117 | — |
| Product | HCID 3610739 | HCID 3610739 | 54.1% |
Reaction Steps
26.2 g (0.137 mol) of 2,5-dichloro-1-nitrobenzene, 20.6 g (0.274 mol) of glycine and 18.9 g (0.137 mol) of potassium carbonate were heated in 200 ml of diethylene glycol at 120° C. for 1 h. After cooling, 100 ml of water were added and the solution was acidified with 1M hydrochloric acid. The precipitate was filtered off with suction. 17.1 g (54%) of the product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849743 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-452f60cafb644a549c11ba456aa5bc05 |
| Source note | uspto-grants-1998_12 |