Lithium Hydroxide → HCID 9807075, compound

HRID 1457568Notes

Reaction equation

C([O:3][C:4]([CH2:6][N:7]1[C:16]2[C:11](=[CH:12][C:13]([N+:37]([O-:39])=[O:38])=[C:14]([N:17]3[CH:21]=[CH:20][C:19]([CH2:22][N:23]4[CH2:28][CH2:27][N:26]([CH2:29][CH2:30][C:31]5[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=5)[CH2:25][CH2:24]4)=[CH:18]3)[CH:15]=2)[NH:10][C:9](=[O:40])[C:8]1=[O:41])=[O:5])C.[OH-].[Li+]>>[C:4]([CH2:6][N:7]1[C:16]2[C:11](=[CH:12][C:13]([N+:37]([O-:39])=[O:38])=[C:14]([N:17]3[CH:21]=[CH:20][C:19]([CH2:22][N:23]4[CH2:28][CH2:27][N:26]([CH2:29][CH2:30][C:31]5[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=5)[CH2:25][CH2:24]4)=[CH:18]3)[CH:15]=2)[NH:10][C:9](=[O:40])[C:8]1=[O:41])([OH:5])=[O:3]

Participants

Reactant 2

HCID 3939Lithium Hydroxide

HCID 22100066HCID 22100066, compound

Product 1

HCID 9807075HCID 9807075, compound

Procedure

20 0.6 g (1.1 mmol) of Example 39 were hydrolyzed with lithium hydroxide as in method 1i.

Sources & evidence

ORD record: ord-a21d92f140de42d0b9cde4304d07af4e
Source dataset: uspto-grants-1998_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05849743

Reaction notes

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