Phenyl Isothiocyanate → HCID 54290112, compound

HRID 1457572Notes

Reaction equation

[NH2:1][C:2]1[CH:3]=[C:4]([C:9]([O:14][CH3:15])=[CH:10][C:11]=1[O:12][CH3:13])[O:5]COC.[C:16]1([N:22]=[C:23]=[S:24])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[C:16]1([NH:22][C:23](=[S:24])[NH:1][C:2]2[CH:3]=[C:4]([OH:5])[C:9]([O:14][CH3:15])=[CH:10][C:11]=2[O:12][CH3:13])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

Reactant 2

HCID 7673Phenyl Isothiocyanate

HCID 22099421HCID 22099421, compound

Product 1

HCID 54290112HCID 54290112, compound

Procedure

(3-Amino-4,6-dimethoxyphenoxy)methoxymethane and phenyl isothiocyanate were treated in the same manner as described in Example 1 to give 3-(3-phenylthioureido)-4,6-dimethoxyphenol (melting point: 152°-154° C.).

Sources & evidence

ORD record: ord-73fbe61c778b40e4aa9a12ec652975e6
Source dataset: uspto-grants-1998_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05849732

Reaction notes

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