Thionyl Chloride → HCID 86753435, compound

HRID 1457644Notes

Reaction equation

HRID 1457644 reaction equation
[C:1]1([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:2]([C:7](O)=[O:8])=[CH:3][CH:4]=[CH:5][CH:6]=1.S(Cl)([Cl:18])=O>>[C:1]1([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:2]([C:7]([Cl:18])=[O:8])=[CH:3][CH:4]=[CH:5][CH:6]=1.[C:1]1([C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 70357o-Phenylbenzoic acid

Product 1

HCID 86753435HCID 86753435, compound

Procedure

A mixture of 5.6 g of [1,1'-biphenyl]-2-carboxylic acid and 29 ml of thionyl chloride is heated on a steam bath for 0.5 hour and the volatiles removed under vacuum. Toluene (40 ml) is added (twice) and the solvent removed under vacuum to give 6.8 g of a yellow oil.

Workup

  1. temperatureis heated on a steam bath for 0.5 hour
  2. customthe volatiles removed under vacuum
  3. additionToluene (40 ml) is added (twice) and the solvent
  4. customremoved under vacuum

Sources & evidence

ORD record
ord-1023000ffd48477588f15d70a4a12069
Source dataset
uspto-grants-1998_12
Patent number
US05849735

Reaction notes

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