HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86753435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | o-Phenylbenzoic acid | HCID 70357 | — |
| Product | HCID 86753435 | HCID 86753435 | — |
Reaction Steps
A mixture of 5.6 g of [1,1'-biphenyl]-2-carboxylic acid and 29 ml of thionyl chloride is heated on a steam bath for 0.5 hour and the volatiles removed under vacuum. Toluene (40 ml) is added (twice) and the solvent removed under vacuum to give 6.8 g of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849735 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-1023000ffd48477588f15d70a4a12069 |
| Source note | uspto-grants-1998_12 |