HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22099546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-(5-Fluoro-2-methylbenzoyl)aminopyridine-3-carbonyl chloride | HCID 15508250 | — |
| Reactant | HCID 22099611 | HCID 22099611 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22099546 | HCID 22099546 | — |
Reaction Steps
As described for Example 1, 6,11-dihydro-5H-pyrido[2,3-b][1,4]benzodiazepine (2 mmol) is reacted with 6-[(5-fluoro-2-methylbenzoyl)amino]pyridine-3-carbonyl chloride (2.1 mmol) in the presence of triethylamine (4 mmol) in dichloromethane to give the product as a solid, m.p. 102° C.-104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849735 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-22a951f5b7e443d7a678962dbb01a0dd |
| Source note | uspto-grants-1998_12 |