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HRID1457918

反应详情

EQUATION

反应方程式

HRID 1457918 的结构方程式

REACTANTS

反应物

3
结构：CI
HCID6328

Methyl iodide

CH3I

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)c1cc(Br)c(O)c(C(C)=O)c1
HCID15818980

Methyl 3-acetyl-5-bromo-4-hydroxybenzoate

C10H9BrO4

PRODUCTS

生成物

1
结构：COC(=O)c1cc(Br)c(OC)c(C(C)=O)c1
HCID22101060

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

1 eq. of methyl 3-acetyl-5-bromo-4-hydroxybenzoate (preparation, see Example 19) was reacted, in acetone, with 2.0 eq. of K2CO3 and 2.1 eq. of methyl iodide to give methyl 3-acetyl-5-bromo-4-methoxybenzoate. Colorless oil, MS (ES): 288 (M+1).