HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 22101154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 22101145 | HCID 22101145 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22101154 | HCID 22101154 | 86.2% |
Reaction Steps
A mixture of the compound of Example 4 (300 mg, 0.7 mmol), DMF (5 ml), methanol (40 ml), and 5% Pd/C (30 mg) was stirred for 24 h under hydrogen. After filtration of the reaction mixture, the filtrate was evaporated under reduced pressure to give the title compound (203 mg, yield 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849779 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-090e7da7844243d882e71cdc4d816db7 |
| Source note | uspto-grants-1998_12 |