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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1458001Generated: November 4, 2026

HCID 22100496, compound → HCID 22100537, compound

https://huagongshe.com/reaction/1458001

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22100496HCID 22100496—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 22100537HCID 22100537—

Reaction Steps

To 1.84 g (5.31 mmol) of 1-benzyloxycarbonyl-3-(1-tert-butoxycarbonylaminocyclopropyl)azetidine dissolved in 100 ml of ethanol was added 1.5 g of 10% palladium-carbon, followed by overnight catalytic hydrogenation at room temperature under normal pressure. After removal of the catalyst by filtration, the solvent was evaporated to yield quantitative amount of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05849757
Source datasetuspto-grants-1998_12
ORD IDord-c6864f1e58214735a2fd9597b6cc5107
Source noteuspto-grants-1998_12