HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22100516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22100512 | HCID 22100512 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22100516 | HCID 22100516 | 100.3% |
Reaction Steps
A mixture of dimethyl 4-(1,1-bis-ethoxycarbonylethyl)-3,5,6-trifluorophthalate (12.9 g, 30.7 mmol), hydrochloric acid (120 ml), and acetic acid (120 ml, was refluxed for 24 h. The reaction mixture was concentrated to dryness to give 9.0 g of the title compound as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05849757 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-400ebc8b6e6643ecb1669f8b8bbbcb70 |
| Source note | uspto-grants-1998_12 |