Water → HCID 85746660, compound

Participants

Reaction Conditions

Reaction Steps

34.9 Grams of isobutylamine is mixed with 50 g of 2,2'-azobis (2-methyl propionate), and 10 g of 28% sodium methoxide solution in methanol is dropwise added thereto with stirring, followed by conducting a reaction at room temperature with stirring for 6 hours and keeping standing overnight. 100 Milliliter of water is added to the reaction solution and cooled to 10° C. to precipitate crystals. The crystals are recovered by filtration and dried to give 56.4 g (yield 83%) of 2,2'-azobis [N-(2 -methylpropyl)-2-methyl propionamide] as pale yellow crystal. The solubility is shown in Table 1.

Provenance & Evidence