Water → HCID 22936069, compound

Participants

Reaction Steps

28.2 Grams of n-hexylamine is mixed with 50 g of 2,2'-azobis (2-methyl propionate), and 20 g of 28% sodium methoxide solution in methanol and 10 ml of methanol are added thereto with stirring followed by conducting a reaction at room temperature with stirring for 6 hours and keeping standing overnight. 100 Milliliter of water is added to the reaction solution and extraction with 100 ml of n-hexane is conducted. The hexane layer is washed with water and dried over anhydrous sodium sulfate. The solvent is removed by distillation to give 76.3 g (yield 95%) of 2,2'-azobis (N-hexyl-2-methyl propionamide) as pale yellow sintering crystal. The solubility is shown in Table 1.

Provenance & Evidence