Water → HCID 22101712, compound

Participants

Reaction Conditions

Reaction Steps

28.3 Grams of propylamine is mixed with 50 g of 2,2'-azobis (2-methyl propionate), and 10 g of 28% sodium methoxide solution in methanol and 10 ml of methanol are added thereto with stirring, followed by conducting a reaction at room temperature with stirring for 6 hours and keeping standing overnight. 100 Milliliter of water is added to the reaction solution and cooled to 5° C. to precipitate crystals. The crystals are recovered by filtration and dried to give 54.0 g (yield: 87%) of 2,2'-azobis(N-propyl-2-methyl propionamide) as pale yellow crystal. The solubility is shown in Table 1.

Provenance & Evidence