HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1458277Generated: November 2, 2026
Sodium methanethiolate → HCID 23283990, compound
https://huagongshe.com/reaction/1458277
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 23283986 | HCID 23283986 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 23283990 | HCID 23283990 | 39.6% |
Reaction Steps
Sodium thiomethoxide (8.97 g) was added to a solution of 2-nitro-4-pentafluorosulphanylbenzonitrile (11.7 g) in acetone and stirred at 20° C. overnight, then evaporated and purified by column chromatography on silica gel eluting with ethyl acetate/hexane (3:97) to give 2-methylthio-4-pentafluorosulphanylbenzonitrile (4.65 g), m.p.101°-1020° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05849928 |
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| Source dataset | uspto-grants-1998_12 |
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| ORD ID | ord-cd2d9228120546eab0f2ebea99c8f5bf |
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| Source note | uspto-grants-1998_12 |
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