HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylamine → HCID 14239709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | Trityl chloride | HCID 6456 | — |
| Reactant | HCID 178519763 | HCID 178519763 | — |
| Product | HCID 14239709 | HCID 14239709 | 60% |
Reaction Steps
This compound was prepared from 3-(hydroxymethyl)-1 H-pyrazole, [J. Am. Chem. Soc, 71, 3996, (1949)], trityl chloride and trimethylamine using the method of Preparation 18, above. The crude product was purified by flash chromatography (gradient elution with hexane/ethyl acetate) to give a white solid (1.428 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05852016 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-b087be63e31642a5a1e6979ccf0645d6 |
| Source note | uspto-grants-1998_12 |