HCID 22096808, compound → HCID 9904129, compound

Participants

Reaction Steps

Methyl 3-methoxy-4-[bis(2-chloroethyl)amino]benzoate (1.0 g; 3.3 mmol) was added to 20 ml of concentrated hydrochloric acid, followed by stirring for 30 minutes under heating and reflux. The solvent was distilled out under reduced pressure, whereby 707 mg of white powder were obtained (yield: 74%).

Provenance & Evidence