HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1458723Generated: October 31, 2026
2-(Ethylamino)ethanol → HCID 22096725, compound
https://huagongshe.com/reaction/1458723
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-(Ethylamino)ethanol | HCID 8072 | — |
| Reactant | 4-Fluorobenzonitrile | HCID 14517 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 22096725 | HCID 22096725 | 21,335.1% |
Reaction Steps
A solution of 10 g (82.6 mmol) of 4-fluorobenzonitrile and 15 g (0.17 mmol) of 2-(ethylamino)ethanol in 30 ml of DMSO was stirred under heat at 140° C. for 3 hours, followed by extraction with ethyl acetate. The solvent was distilled out under reduced pressure, followed by washing with ethyl acetate, whereby 6.9 g of white powder were obtained (yield: 44%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05852011 |
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| Source dataset | uspto-grants-1998_12 |
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| ORD ID | ord-fe415d2f191c412ea92a4e45fcc88562 |
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| Source note | uspto-grants-1998_12 |
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