HRID1458797

反应详情

EQUATION

反应方程式

HRID 1458797 的结构方程式

PROCEDURE

实验过程

28 g (0.11 mol) of 2-cyclohexylamino-5-trifluoromethylaniline and 322 g (2.2 mol) of diethyl oxalate were refluxed for 2 hours. The reaction mixture was then concentrated, and the crude product was recrystallized from ethanol.

WORKUP

后处理

  1. concentrationThe reaction mixture was then concentrated
  2. customthe crude product was recrystallized from ethanol