Hydrochloric Acid → HCID 178499561, compound

HRID 1458970Notes

Reaction equation

HRID 1458970 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (4.00 g, 24.6 mmol) in methanol (100 ml) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature (RT) for 18 hr. The solvent was evaporated in vacuo to afford the title compound as a solid.

Workup

  1. customto stand at room temperature
  2. custom(RT)
  3. customfor 18 hr
  4. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-f25363beb2fb44eeb8bc79b8e0a78b6b
Source dataset
uspto-grants-1998_12
Patent number
US05852010

Reaction notes

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