Ammonium Chloride → HCID 178425543, compound

HRID 1459191Notes

Reaction equation

HRID 1459191 reaction equation
CO[C:3]1[CH2:4][C:5]([CH3:11])([CH3:10])[CH2:6][CH2:7][CH2:8][N:9]=1.[Cl-:12].[NH4+:13]>CCO>[ClH:12].[CH3:10][C:5]1([CH3:11])[CH2:6][CH2:7][CH2:8][NH:9][C:3](=[NH:13])[CH2:4]1

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 18428630HCID 18428630, compound

Product 1

HCID 178425543HCID 178425543, compoundYield 61.6%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product of EXAMPLE 64 (260 mg, 1.7 mmol) in 10 mL of EtOH was reacted with ammonium chloride (88 mg, 1.7 mmol) by the method of EXAMPLE 27 to yield 185 mg (55%) of the title material.

Sources & evidence

ORD record
ord-1d8dcaf0f52b41648fa9e07239589a3b
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

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