HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178425543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 7-Methoxy-5,5-dimethyl-2,3,4,6-tetrahydroazepine | HCID 18428630 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178425543 | HCID 178425543 | 61.6% |
Reaction Steps
The product of EXAMPLE 64 (260 mg, 1.7 mmol) in 10 mL of EtOH was reacted with ammonium chloride (88 mg, 1.7 mmol) by the method of EXAMPLE 27 to yield 185 mg (55%) of the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05854234 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-1d8dcaf0f52b41648fa9e07239589a3b |
| Source note | uspto-grants-1998_12 |