Ammonium Chloride → HCID 178439094, compound

HRID 1459201Notes

Reaction equation

HRID 1459201 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH2:10][CH:11]=[CH2:12])[N:9]=1.[Cl-:13].[NH4+:14]>CO>[ClH:13].[CH2:10]([CH:8]1[NH:9][C:3](=[NH:14])[CH2:4][CH2:5][CH2:6][CH2:7]1)[CH:11]=[CH2:12]

Participants

4

Reactant 2

HCID 25517Ammonium ChlorideHCID 107734033,4,5,6-Tetrahydro-7-methoxy-2-(2-propenyl)-2h-azepine

Product 1

HCID 178439094HCID 178439094, compoundYield 79.5%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The product of EXAMPLE 106 (70 mg, 0.42 mmol) in 3 mL of MeOH was reacted with ammonium chloride (21.4 mg, 0.4 mmol) by the method of EXAMPLE 27 to yield 60 mg (76%) of the title material.

Sources & evidence

ORD record
ord-93727c32a3a74cfa8533953e5163751d
Source dataset
uspto-grants-1998_12
Patent number
US05854234

Reaction notes

Loading…