HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178439094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 3,4,5,6-Tetrahydro-7-methoxy-2-(2-propenyl)-2h-azepine | HCID 10773403 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178439094 | HCID 178439094 | 79.5% |
Reaction Steps
The product of EXAMPLE 106 (70 mg, 0.42 mmol) in 3 mL of MeOH was reacted with ammonium chloride (21.4 mg, 0.4 mmol) by the method of EXAMPLE 27 to yield 60 mg (76%) of the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05854234 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-93727c32a3a74cfa8533953e5163751d |
| Source note | uspto-grants-1998_12 |