HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54201469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 54030760 | HCID 54030760 | — |
| Product | HCID 54201469 | HCID 54201469 | — |
Reaction Steps
N-(10,11-Dihydro-5H-dibenzo(b,e)(1,4)diazepin-6-yl)-4-methoxybenzensulfonamide, which had been synthesized in the same manner as the one of Example 31, was reacted with acetic anhydride at room temperature. Then the obtained product was purified by silica gel column chromatography and thus the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05854274 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-422d9deff1bb46e693a5f634ec9f9b72 |
| Source note | uspto-grants-1998_12 |