HRID1460066

反应详情

EQUATION

反应方程式

HRID 1460066 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared by treatment of 4,6-dichloro-5-nitropyrimidine with N-benzylphenylethylamine, followed by reaction with 2-(1 H-imidazol-1 -yl)-methylimidazole, reduction with tin (II) chloride, cyclization with carbonyidiimidazole, and hydrogenation with palladium on carbon in ethanol containing 1.1 eq. NaOH at 50 psi and 50° C.

WORKUP

后处理

  1. customat 50 psi and 50° C.