HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 15067105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Glycol monoethyl ether | HCID 8076 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15067105 | HCID 15067105 | — |
Reaction Steps
To 30g of 2-ethoxyethanol in 300ml of tetrahydrofuran 27.4ml of pyridine were added and 26.4ml of mesyl chloride added dropwise at room temperature over 15 minutes. The mixture was refluxed overnight, the solid that formed filtered off and the solvent evaporated off from the residue. The residue was distilled under 20m Hg to give 2-ethoxyethyl methanesulphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071468 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-f8da1dc8ee6d42478c217b4800fba461 |
| Source note | uspto-grants-1991_12 |