反应详情

To 30g of 2-ethoxyethanol in 300ml of tetrahydrofuran 27.4ml of pyridine were added and 26.4ml of mesyl chloride added dropwise at room temperature over 15 minutes. The mixture was refluxed overnight, the solid that formed filtered off and the solvent evaporated off from the residue. The residue was distilled under 20m Hg to give 2-ethoxyethyl methanesulphonate.

1. temperatureThe mixture was refluxed overnight
2. customthe solid that formed
3. filtrationfiltered off
4. customthe solvent evaporated off from the residue
5. distillationThe residue was distilled under 20m Hg