HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 3-benzyl-2-(1-methylpiperidin-3-yl)-3H-imidazo [4,5-b] pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | HCID 178480253 | HCID 178480253 | — |
| Product | 3-benzyl-2-(1-methylpiperidin-3-yl)-3H-imidazo [4,5-b] pyridine | HCID 21647627 | — |
Reaction Steps
Operation is carried out similarly to the description of Example 5 with the difference that 2-(1-methylpiperidin-3-yl)3H-imidazo [4,5-b] pyridine is reacted with benzylchloride to obtain 3-benzyl-2-(1-methylpiperidin-3-yl)-3H-imidazo [4,5-b] pyridine as an oil, after purification by chromatography on silicagel column (CHCl3 -CH3OH 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071855 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-fa99d04252cc43818c927e1228b73094 |
| Source note | uspto-grants-1991_12 |