HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19801133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 19107050 | HCID 19107050 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 19801133 | HCID 19801133 | 81% |
Reaction Steps
A solution of the compound from Example 36 (0.65 g, 2.4 mmol) was reduced in a suspension of lithium aluminum hydride in ether as described in Example 33. A solution of the free amine in diethyl ether was treated with isopropanolic HCl to give the title compound (0.51 g, 81%), mp 248°-249° c.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071853 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-99f3d9a998064254a7fdfc57f87c13e8 |
| Source note | uspto-grants-1991_12 |