Triethylamine → HCID 9867956, compound

HRID 1460637Notes

Reaction equation

HRID 1460637 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH2:9][CH3:10])[C:4]=1[NH:11][C:12](=[O:15])[CH:13]=[CH2:14])[CH3:2].[CH3:16][C:17]([C:20]1[CH:25]=[C:24]([SH:26])[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]=1[OH:31])([CH3:19])[CH3:18].C(N(CC)CC)C>CO>[CH3:30][C:27]([C:22]1[CH:23]=[C:24]([S:26][CH2:14][CH2:13][C:12]([NH:11][C:4]2[C:5]([CH2:9][CH3:10])=[CH:6][CH:7]=[CH:8][C:3]=2[CH2:1][CH3:2])=[O:15])[CH:25]=[C:20]([C:17]([CH3:19])([CH3:18])[CH3:16])[C:21]=1[OH:31])([CH3:28])[CH3:29]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 703702,6-Di-tert-butyl-4-mercaptophenolHCID 15680271HCID 15680271, compound

Product 1

HCID 9867956HCID 9867956, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound was prepared by the method of Example 4 from N-(2,6-diethylphenyl)-2-propenamide (1.01 g, 0.005 mole), 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (1.19 g, 0.005 mole) and triethylamine (0.5 ml) in methanol, m.p. ca. 150.5°-151.5° C.

Sources & evidence

ORD record
ord-6650b4ba68ed48af8e75fbf4e5a9dde1
Source dataset
uspto-grants-1991_12
Patent number
US05071876

Reaction notes

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