N-Phenylglycine → HCID 19100958, compound

HRID 1460755Notes

Reaction equation

HRID 1460755 reaction equation
[CH2:1]([N:4]([CH2:10][CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].[C:13]1([NH:19][CH2:20]C(O)=O)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C1(C)C=CC=CC=1>[C:13]1([N:19]2[CH2:20][CH2:3][CH:2]3[CH:11]2[CH2:10][N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]3)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 66025N-PhenylglycineHCID 11084330Ethyl allyl(2-oxoethyl)carbamate

Product 1

HCID 19100958HCID 19100958, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate and 7.6 50 mmol) of phenylglycine are heated under reflux overnight in 200 ml of toluene. The mixture is decanted from resinous material and concentrated, and the residue is distilled.

Workup

  1. customThe mixture is decanted from resinous material
  2. concentrationconcentrated
  3. distillationthe residue is distilled

Sources & evidence

ORD record
ord-1fff63c7ccf74cd0a9ac9d39ead9c353
Source dataset
uspto-grants-1991_12
Patent number
US05071999

Reaction notes

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