HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenylglycine → HCID 19100958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenylglycine | HCID 66025 | — |
| Reactant | Ethyl allyl(2-oxoethyl)carbamate | HCID 11084330 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19100958 | HCID 19100958 | — |
Reaction Steps
8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate and 7.6 50 mmol) of phenylglycine are heated under reflux overnight in 200 ml of toluene. The mixture is decanted from resinous material and concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071999 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-1fff63c7ccf74cd0a9ac9d39ead9c353 |
| Source note | uspto-grants-1991_12 |