HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19100973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sarcosine | HCID 1088 | — |
| Reactant | HCID 19738514 | HCID 19738514 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19100973 | HCID 19100973 | — |
Reaction Steps
9.1 g (43 mmol) of ethyl N-(2-fluoromethylallyl) -N-(2-oxoethyl)-carbamate are heated under reflux overnight in a water separator with 3.9 g (43 mmol) of powdered sarcosine in 170 ml of toluene. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071999 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-46ed80427eb24ea4bca35732ffcf7b0c |
| Source note | uspto-grants-1991_12 |