HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 19100964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | N-Benzylglycine ethyl ester | HCID 80908 | — |
| Reactant | Ethyl allyl(2-oxoethyl)carbamate | HCID 11084330 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19100964 | HCID 19100964 | — |
Reaction Steps
50 g (0.25 mol) of N-benzylglycine ethyl ester in 1 1 of toluene are heated under reflux in a water separator and 43 g (0.25 mol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate are added dropwise during the course of two hours. The mixture is heated under reflux until water no longer separates and concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071999 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-5698b08720e74971810df6f41f337fa5 |
| Source note | uspto-grants-1991_12 |