HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Heptanoate → heptanohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Heptanoate | HCID 7797 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | heptanohydrazide | HCID 240032 | 51.2% |
Reaction Steps
12.2 g of hydrazine hydrate was added to a solution of 15 g of ethyl heptanoate in 20 ml of ethanol, followed by heat-refluxing for 4.5 hours. After the reaction, the reaction mixture was cooled to precipitate a crystal. The crystal was recovered by filtration and recrystallized from 20 ml of ethanol to obtain 7 g of heptanohydrazide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075030 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-46b2d9783d724d0cbfad6567f034ef7a |
| Source note | uspto-grants-1991_12 |