HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 19980406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19980412 | HCID 19980412 | — |
| Solvent | Water methylene chloride | HCID 21908982 | — |
| Product | HCID 19980406 | HCID 19980406 | — |
Reaction Steps
The product of step b) (1.50 g, 0.0066 mmol), 50% NaOH (15 ml) and THF (20 ml) were mixed and stirred overnight. The reaction mixture was diluted with CH2Cl2 /H2O and separated. The aqueous layer was further extracted with CH2Cl2 (50 ml×2) and worked-up to give 1.42 g of a tan oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075317 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-1d26daba559a435ba446700a9b7c0ac7 |
| Source note | uspto-grants-1991_12 |