Hydroxyamine hydrochloride → HCID 72742956, compound

HRID 1461339Notes

Reaction equation

HRID 1461339 reaction equation
[CH3:1][N:2]1[CH2:12][CH2:11][C:5]2([O:9][CH2:8][C:7](=O)[CH2:6]2)[CH2:4][CH2:3]1.Cl.[NH2:14][OH:15]>CO>[CH3:1][N:2]1[CH2:12][CH2:11][C:5]2([O:9][CH2:8][C:7](=[N:14][OH:15])[CH2:6]2)[CH2:4][CH2:3]1

Participants

4

Reactant 2

HCID 443297Hydroxyamine hydrochlorideHCID 10352099HCID 10352099, compound

Product 1

HCID 72742956HCID 72742956, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of Example 3 (0.6 g, 3.5 mmol) was dissolved in methanol (50 ml) and placed under nitrogen. Hydroxylamine hydrochloride was added and the reaction was stirred at room temperature overnight.

Sources & evidence

ORD record
ord-a9e530da9fe84a2395e240b6243b4118
Source dataset
uspto-grants-1991_12
Patent number
US05075317

Reaction notes

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