Potassium Carbonate → HCID 178449885, compound

Participants

Reaction Steps

To a stirred mixture of N-ferrocenoyl-N'-tert-butylhydrazine (0.5 g, 1.65 mmoL) in toluene (10 mL), and potassium carbonate (0.5 g, 3.62 mmoL) in water (5 ml) was added a solution of 2-bromobenzoyl chloride (0.5 g, 1.82 mmoL) in toluene (5 mL) dropwise in 15 minutes. The resulting mixture was stirred vigorously for two hours and the solid was filtered, washed with water, ethyl ether and dried to afford product as a bright yellow solid, melting point 175° C.

Provenance & Evidence