HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19742191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Octadecanethiol | HCID 17905 | — |
| Reactant | HCID 19742171 | HCID 19742171 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19742191 | HCID 19742191 | 30.9% |
Reaction Steps
The procedure of Example 10 is repeated using 8.72 g (28.5 mmol) of 1-isobutyl-2,8-dichloro-3,7,9-trioxa-1-aza-2,8-diphosphaspiro[4.5]decane, 16.33 g (57 mmol) of n-octadecyl mercaptan and 8.74 mL (63 mmol) of triethylamine in 200 mL of toluene. A white solid (7.11 g) is isolated. The product is identified by mass spectroscopy: m/z=805.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075482 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-a20cca4e709d4fa4886b459d9c4e8095 |
| Source note | uspto-grants-1991_12 |