Sodium aminomethanesulfonate → HCID 86745351, compound

Participants

Reaction Steps

A four-necked flask fitted with stirrer and condenser means was charged with 39.8 g of lauryltrihydroxyethylammonium bromide, 15.9 g of sodium aminomethanesulfonate and 200 g of isopropyl alcohol and the reaction was conducted at 70°-80° C. in an atmosphere of nitrogen gas introduced at a low flow rate for 5 hours. The precipitate was then filtered off and the filtrate was concentrated. The residue was dissolved in 200 g of isopropyl alcohol and the insolubles were filtered off. Finally, the filtrate was concentrated to give 40.1 g (theoretical yield 42.8 g) of lauryltrihydroxyethylammonium aminomethanesulfonate as a waxy product. The elemental analysis is shown below.

Provenance & Evidence