Ethyl Acrylate → HCID 15754165, compound

HRID 1461668Notes

Reaction equation

HRID 1461668 reaction equation
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[CH3:8][C:9]([NH2:17])([CH3:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH3:8][C:9]([NH:17][CH2:3][CH2:2][C:1]([O:5][CH2:6][CH3:7])=[O:4])([CH3:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 68509Cumylamine

Product 1

HCID 15754165HCID 15754165, compoundYield 77.8%

Conditions

Temperature
100 °C

Procedure

100 g (1 mol) of ethyl acrylate was added to 135.2 g (1 mol) of α,α-dimethylbenzylamine, and the mixture was stirred at 100° C. for 18 hours. The reaction product was subjected to distillation to obtain 180.7 g (yield: 77.8%) of the desired compound.

Workup

  1. distillationThe reaction product was subjected to distillation

Sources & evidence

ORD record
ord-bf85e2d5ad5c4e5e9a19290a28b4b63f
Source dataset
uspto-grants-1991_12
Patent number
US05076834

Reaction notes

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