HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 14851349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Azacyclonol | HCID 15723 | — |
| Reactant | 4-(2-Chloroethyl)phenyl methyl ether | HCID 87513 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14851349 | HCID 14851349 | — |
Reaction Steps
A mixture of 4 g of α,α-diphenyl-4-piperidinomethanol, 0.94 g of powdered potassium hydroxide and 200 mg of KI are dispersed in 50 ml of toluene in a 250 ml round-bottomed flask. Addition of 2.3 ml of 4-methoxyphenylethyl chloride is followed by heating under reflux for 3 days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05077301 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-612bd3f9f92541a79a3d4b64bffe5a14 |
| Source note | uspto-grants-1991_12 |