HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 178432285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 14674208 | HCID 14674208 | — |
| Reactant | HCID 178432280 | HCID 178432280 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 178432285 | HCID 178432285 | 35% |
Reaction Steps
The compound obtained in Stage F, 9.7 g of 3-(2-chloroethyl)-8-cyano-4-hydroxy-2-methylimidazo[1,5-a]-pyrimidine, 23 g of sodium carbonate, 0.5 g of potassium iodide and 800 ml of 4-methyl-2-pentanone are brought to reflux. The procedure then adopted is as described in Example 1, Stage C, to obtain the expected hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05077288 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-4ab95b1d342244bdb45a25a5dccb4b52 |
| Source note | uspto-grants-1991_12 |